Possible spoilers in here. You've been warned.
My three are:
1. Mr. Freeze (Arkham City). This one was clever, particularly on New Game Plus.
2. Firefly (Arkham Origins). It's like Poison Ivy except he's more dodge-y, the bridge makes for a bigger arena, and grappling onto him is plain badass.
3. Killer Croc (Arkham Asylum). OK, so it's not really a boss battle so much as survive the maze, but that's IMO the beauty of it. Croc was a real tough guy in this game, and it made for a memorable experience.
Thoughts?
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